Журналы →  Chernye Metally →  2017 →  №12 →  Назад

Metal Acience and Metallography
Название Examination of crystal structure of steels 32G1, 32G2 and 32 KhGF via EBSD-analysis
Автор M. A. Borovykh, O. A. Chikova, V. V. Vyukhin
Информация об авторе

Ural State Federal University named after B. N. Eltsin (Ekaterinburg, Russia):

Borovykh M. A., Post-graduate, Chair of Physics, e-mail: makboro@e1.ru
Chikova O. A., Dr. Eng., Prof., Chair of Physics, e-mail: chik63@mail.ru
Vyukhin V. V., Cand. Eng., Senior Researcher, Scientific Center of Physics of Metal Liquids, e-mail: v.v.vyukhin@urfu.ru

Реферат

The results of examination of the crystal of structure of samples made of 32G1, 32G2 and 35HGF are presented. These samples were selected from hot-rolled pipes in the conditions of Sinarsky pipe plant. The steel study was conducted to justify the selection of the steel grade on the basis of the relationships «structure-properties». The method of EBSD analysis (Electron Backscatter Diffraction) has been used for this purpose. The size of effective ferrite grain and orientation of the crystallites are determined; information about local mechanical stresses according to the cards of the Taylor and Schmid factors is obtained. It was found that arising of local distortions in metal crystal lattice and large-angle (non-special) crystal boundaries are the cause of development of inter-crystalline corrosion in the examined ferrite steels. Heat treatment procedure has the effect on grain size and histogram of crystalline disorientation. It is concluded that fine grain, large proportion of low-angle grain boundaries, less local mechanical stress, and, therefore, high plasticity and high corrosion resistance relating to hydrocarbons are typical for steel grade 32G2.

Ключевые слова Steel, crystal structure, EBSD-analysis, small-angle grain boundaries, Taylor factor, Schmid factor
Библиографический список

1. Goldshteyn M. I., Grachev S. V., Veksler Yu. G. Special steels. Moscow : MISIS, 1999. 408 p.
2. Steels and alloys. Grade guide : reference edition. Moscow : Intermet engineering, 2001. 608 p.
3. Structure and corrosion of metals and alloys. Metallurgy. Moscow, 1989. 400 p.
4. GOST R 9.905-2007. Unified system of corrosion and ageing protection. Corrosion test methods. General requirements. Moscow : Standartinform, 2007. 18 p.
5. GOST 9.908-85. Unified system of corrosion and ageing protection. Metals and alloys. Methods for determination of corrosion and corrosion resistance indices. Moscow : Izdatelstvo standartov, 1999. 16 p.
6. Danilenko V. N., Mironov S. Yu., Belyakov A. N., Zhilyaev A. P. Application of EBSD Analysis of Material Physics (Review). Zavodskaya laboratoriya. Diagnostika materialov. 2012. No. 2, Vol. 78. pp. 28–46.
7. Difraction method of reflected electrons in materials science. Ed.: A. Shvarts, M. Kumar, B. Adams, D. Fild. Moscow : Tekhnosfera, 2014. 544 p.
8. Saeidi N., Ashrafi zadeh F., Niroumand B., Barlat F. EBSD Study of Damage Mechanisms in a High-Strength Ferrite-Martensite Dual-Phase Steel. Journal of Materials Engineering and Performance. 2015. Vol. 24, Iss. 1. pp. 53–58.
9. Belonosov A. V., Chikova O. A., Yurovskikh V. V., Chezganov D. S. Examining the structure of mill rolls made of 9X2MΦ and 8X3CΓΦ steels using the ultrasonic method for quality control. Defektoskopiya. 2013. No. 4. pp. 17–28.
10. Nohava J., Hausild P., Karlık M., Bompard P. Electron backscattering diffraction analysis of secondary cleavage cracks in a reactor pressure vessel steel. Materials Characterization. 2003. 49. pp. 211–217.
11. Watanabe K., Matsuda K., Miura N., Uetani Y. Ikeno S., Yoshida T., Murakami S. Characteristics of grain boundaries on intergranular fractured Al-Zn-Mg alloy aged at peak condition – Keikinzoku. Journal of Japan Institute of Light Metals. 2014. Vol. 64, Iss. 8. pp. 368–372.
12. Helmut Mehrer. Diffusion in Solids. Dolgoprudnyy : Izdateskiy dom «Intellekt», 2011. 536 p.
13. Lin P., Palumbo G., Erb U., Aust K. T. Influence of grain boundary character distribution on sensitization and intergranular corrosion of alloy 600. Scripta Metallurgica et Materialia. 1995. Vol. 33, Iss. 9. pp. 1387–1392.
14. Palumbo G., King P. J., Aust K. T., Erb U., Lichtenberger P. C. Grain boundary design and control for intergranular stress-corrosion resistance. Scripta Metallurgica et Materialia. 1991. Vol. 25. pp. 1775–1780.
15. Bennett B. W., Pickering H. W. Effect of grain boundary structure on sensitization and corrosion of stainless steel. Metallurgical Transactopns. 1985. Vol. 18. A. pp. 1117–1124.
16. Lopatin N. V. Microstructure evolution in pure titanium during warm deformation by combined rolling processes. Materials Science and Engineering: A. 2012. Vol. 556. pp. 704–715.
17. Fukuya K., Nishioka H., Fujii K., Miura T., Torimaru T. An EBSD examination of SUS316 stainless steel irradiated to 73 dpa and deformed at 593 K. Journal of Nuclear Materials. 2011. Vol. 417, Iss. 1-3. pp. 958–962.
18. Masoumi M., Santos L. P. M., Bastos I. N., Tavares S. S. M., da Silva M. J. G., de Abreu H. F. G. Texture and grain boundary study in high strength Fe-18Ni-Co steel related to hydrogen embrittlement. Materials and Design. 2016. Vol. 91. pp. 90–97.
19. Mohtadi-Bonab M. A., Szpunar J. A., Basu R., Eskandari M. The mechanism of failure by hydrogen induced cracking in an acidic environment for API 5L X70 pipeline steel. International Journal of Hydrogen Energy. 2015. Vol. 40, Iss. 2. pp. 1096–1107.
20. Yu X., Jiang Z., Zhao J., Wei D., Zhou C., Huang Q. Microstructure and micro texture evolutions of deformed oxide layers on a hot-rolled micro alloyed steel. Corrosion Science. 2015. Vol. 90. pp. 140–152.

Language of full-text русский
Полный текст статьи Получить
Назад